CEN CEN/TS 16621 Food analysis - Determination of benzo[a]pyrene, benz[a]anthracene, chrysene and benzo[b]fluoranthene in foodstuffs by high performance liquid chromatography with fluorescence detection (HPLC-FD)
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- Техэксперт: Машиностроительный комплекс
- Картотека зарубежных и международных стандартов
- BSI BS EN ISO 18395 Animal and vegetable fats and oils - Determination of monoacylglycerols, diacylglycerols, triacylglycerols and glycerol by high-performance size-exclusion chromatography (HPSEC) - AMD 17391: October 31, 2007
- BSI BS EN ISO 661 Animal and vegetable fats and oils - Preparation of test sample - CORR 17492: December 31, 2007
- BSI BS EN ISO 15304 Animal and Vegetable Fats and Oils - Determination of the Content of Trans Fatty Acid Isomers of Vegetable Fats and Oils - Gas Chromatographic Method - CORR 13913: May 14, 2002; CORR 15728: June 2006
- ISO 661 Animal and vegetable fats and oils Preparation of test sample - Third Edition
- ISO 22959 Animal and vegetable fats and oils — Determination of polycyclic aromatic hydrocarbons by on-line donor-acceptor complex chromatography and HPLC with fluorescence detection - First Edition
- ISO 661 Animal and vegetable fats and oils Preparation of test sample - Third Edition
- BSI BS EN ISO 15304 Animal and Vegetable Fats and Oils - Determination of the Content of Trans Fatty Acid Isomers of Vegetable Fats and Oils - Gas Chromatographic Method - CORR 13913: May 14, 2002; CORR 15728: June 2006
- BSI BS EN ISO 661 Animal and vegetable fats and oils - Preparation of test sample - CORR 17492: December 31, 2007
- 67
- BSI BS EN ISO 18395 Animal and vegetable fats and oils - Determination of monoacylglycerols, diacylglycerols, triacylglycerols and glycerol by high-performance size-exclusion chromatography (HPSEC) - AMD 17391: October 31, 2007
- BSI BS EN ISO 661 Animal and vegetable fats and oils - Preparation of test sample - CORR 17492: December 31, 2007
- BSI BS EN ISO 15304 Animal and Vegetable Fats and Oils - Determination of the Content of Trans Fatty Acid Isomers of Vegetable Fats and Oils - Gas Chromatographic Method - CORR 13913: May 14, 2002; CORR 15728: June 2006
- ISO 661 Animal and vegetable fats and oils Preparation of test sample - Third Edition
- ISO 22959 Animal and vegetable fats and oils — Determination of polycyclic aromatic hydrocarbons by on-line donor-acceptor complex chromatography and HPLC with fluorescence detection - First Edition
- ISO 661 Animal and vegetable fats and oils Preparation of test sample - Third Edition
- BSI BS EN ISO 15304 Animal and Vegetable Fats and Oils - Determination of the Content of Trans Fatty Acid Isomers of Vegetable Fats and Oils - Gas Chromatographic Method - CORR 13913: May 14, 2002; CORR 15728: June 2006
- BSI BS EN ISO 661 Animal and vegetable fats and oils - Preparation of test sample - CORR 17492: December 31, 2007
- 67.200
- BSI BS EN ISO 18395 Animal and vegetable fats and oils - Determination of monoacylglycerols, diacylglycerols, triacylglycerols and glycerol by high-performance size-exclusion chromatography (HPSEC) - AMD 17391: October 31, 2007
- BSI BS EN ISO 661 Animal and vegetable fats and oils - Preparation of test sample - CORR 17492: December 31, 2007
- BSI BS EN ISO 15304 Animal and Vegetable Fats and Oils - Determination of the Content of Trans Fatty Acid Isomers of Vegetable Fats and Oils - Gas Chromatographic Method - CORR 13913: May 14, 2002; CORR 15728: June 2006
- ISO 661 Animal and vegetable fats and oils Preparation of test sample - Third Edition
- ISO 22959 Animal and vegetable fats and oils — Determination of polycyclic aromatic hydrocarbons by on-line donor-acceptor complex chromatography and HPLC with fluorescence detection - First Edition
- ISO 661 Animal and vegetable fats and oils Preparation of test sample - Third Edition
- BSI BS EN ISO 15304 Animal and Vegetable Fats and Oils - Determination of the Content of Trans Fatty Acid Isomers of Vegetable Fats and Oils - Gas Chromatographic Method - CORR 13913: May 14, 2002; CORR 15728: June 2006
- BSI BS EN ISO 661 Animal and vegetable fats and oils - Preparation of test sample - CORR 17492: December 31, 2007
- 67.200.10
- BSI BS EN ISO 18395 Animal and vegetable fats and oils - Determination of monoacylglycerols, diacylglycerols, triacylglycerols and glycerol by high-performance size-exclusion chromatography (HPSEC) - AMD 17391: October 31, 2007
- BSI BS EN ISO 661 Animal and vegetable fats and oils - Preparation of test sample - CORR 17492: December 31, 2007
- BSI BS EN ISO 15304 Animal and Vegetable Fats and Oils - Determination of the Content of Trans Fatty Acid Isomers of Vegetable Fats and Oils - Gas Chromatographic Method - CORR 13913: May 14, 2002; CORR 15728: June 2006
- ISO 661 Animal and vegetable fats and oils Preparation of test sample - Third Edition
- ISO 22959 Animal and vegetable fats and oils — Determination of polycyclic aromatic hydrocarbons by on-line donor-acceptor complex chromatography and HPLC with fluorescence detection - First Edition
- ISO 661 Animal and vegetable fats and oils Preparation of test sample - Third Edition
- BSI BS EN ISO 15304 Animal and Vegetable Fats and Oils - Determination of the Content of Trans Fatty Acid Isomers of Vegetable Fats and Oils - Gas Chromatographic Method - CORR 13913: May 14, 2002; CORR 15728: June 2006
- BSI BS EN ISO 661 Animal and vegetable fats and oils - Preparation of test sample - CORR 17492: December 31, 2007
- BSI BS EN ISO 18395 Animal and vegetable fats and oils - Determination of monoacylglycerols, diacylglycerols, triacylglycerols and glycerol by high-performance size-exclusion chromatography (HPSEC) - AMD 17391: October 31, 2007
- BSI BS EN ISO 18395 Animal and vegetable fats and oils - Determination of monoacylglycerols, diacylglycerols, triacylglycerols and glycerol by high-performance size-exclusion chromatography (HPSEC) - AMD 17391: October 31, 2007
- BSI BS EN ISO 18395 Animal and vegetable fats and oils - Determination of monoacylglycerols, diacylglycerols, triacylglycerols and glycerol by high-performance size-exclusion chromatography (HPSEC) - AMD 17391: October 31, 2007
- BSI BS EN ISO 661 Animal and vegetable fats and oils - Preparation of test sample - CORR 17492: December 31, 2007
- BSI BS EN ISO 15304 Animal and Vegetable Fats and Oils - Determination of the Content of Trans Fatty Acid Isomers of Vegetable Fats and Oils - Gas Chromatographic Method - CORR 13913: May 14, 2002; CORR 15728: June 2006
- ISO 661 Animal and vegetable fats and oils Preparation of test sample - Third Edition
- ISO 22959 Animal and vegetable fats and oils — Determination of polycyclic aromatic hydrocarbons by on-line donor-acceptor complex chromatography and HPLC with fluorescence detection - First Edition
- ISO 661 Animal and vegetable fats and oils Preparation of test sample - Third Edition
- BSI BS EN ISO 15304 Animal and Vegetable Fats and Oils - Determination of the Content of Trans Fatty Acid Isomers of Vegetable Fats and Oils - Gas Chromatographic Method - CORR 13913: May 14, 2002; CORR 15728: June 2006
- BSI BS EN ISO 15304 Animal and Vegetable Fats and Oils - Determination of the Content of Trans Fatty Acid Isomers of Vegetable Fats and Oils - Gas Chromatographic Method - CORR 13913: May 14, 2002; CORR 15728: June 2006
- ISO 661 Animal and vegetable fats and oils Preparation of test sample - Third Edition
- ISO 22959 Animal and vegetable fats and oils — Determination of polycyclic aromatic hydrocarbons by on-line donor-acceptor complex chromatography and HPLC with fluorescence detection - First Edition
- ISO 661 Animal and vegetable fats and oils Preparation of test sample - Third Edition
- ISO 22959 Animal and vegetable fats and oils — Determination of polycyclic aromatic hydrocarbons by on-line donor-acceptor complex chromatography and HPLC with fluorescence detection - First Edition
- CEN EN 16619 Food analysis - Determination of benzo[a]pyrene, benz[a]anthracene, chrysene and benzo[b]fluoranthene in foodstuffs by gas chromatography mass spectrometry (GC-MS)
- CEN EN ISO 22959 Animal and vegetable fats and oils - Determination of polycyclic aromatic hydrocarbons by on-line donor-acceptor complex chromatography and HPLC with fluorescence detection
- BSI BS EN ISO 18395 Animal and vegetable fats and oils - Determination of monoacylglycerols, diacylglycerols, triacylglycerols and glycerol by high-performance size-exclusion chromatography (HPSEC) - AMD 17391: October 31, 2007
- Картотека зарубежных и международных стандартов
European Committee for Standardization
Food analysis - Determination of benzo[a]pyrene, benz[a]anthracene, chrysene and benzo[b]fluoranthene in foodstuffs by high performance liquid chromatography with fluorescence detection (HPLC-FD)
N CEN/TS 16621
Annotation
This Technical Specification specifies a method for the determination of benzo[a]pyrene (BaP) plus benz[a]anthracene (BaA), benzo[b]fluoranthene (BbF) and chrysene (CHR) in several food matrices. The method is based on size exclusion chromatography (SEC) cleanup, followed by quantification with high performance liquid chromatography (HPLC) with programmable fluorescence detection. This method has been in-house validated via the analysis of spiked samples of edible olive oil, fresh mussels, smoked fish, smoked meat products, processed cereal-based foods for young children, infant formulae, chocolate and food supplements (isoflavones) at levels ranging from 0,25 g/kg to 1,00 g/kg and from 4,95 g/kg to 23,53 g/kg, depending on the Polycyclic Aromatic Hydrocarbon (PAH) or the matrix. This method complies with the performance characteristics specified for BaP, BaA, BbF and CHR in current legislation [3].
The method has been shown to be applicable to a variety of additional matrices as meat products, fresh fish, paprika, roasted coffee, bread, herbs, breakfast cereals, beer, sunflower oil, olives and fried tomato, with a limit of quantification below 0,5 g/kg.
In addition, the method was tested in-house and shown to be applicable also for the quantification of the other 12 PAHs of the 15+1 EU priority PAHs set (benzo[c]fluorene (BcL), benzo[j]fluoranthene (BjF), benzo[k]fluoranthene (BkF), cyclopenta[cd]pyrene (CPP), dibenz[a,h]anthracene (DhA), dibenzo[a,e]pyrene (DeP), benzo[ghi]perylene (BgP), dibenzo[a,h]pyrene (DhP), dibenzo[a,i]pyrene (DiP), dibenzo[a,l]pyrene (DlP), indeno[1,2,3-cd]pyrene (IcP), 5-methylchrysene (5MC)) in all matrices listed above and at similar level ranges, except for CPP, where a UV detection had to be used with limits of quantification above 8 g/kg.
